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Differential Scanning Calorimetry High Precision Laboratory Thermal Analyzer Closed Furnace Automatic Combustion Calorimeter

Differential Scanning Calorimetry (DSC) is primarily used to measure heat-related physical and chemical changes, such as glass transition temperature, melting point, melting temperature, heat of crystallization, heat of phase transition reaction, thermal stability of products, curing/crosslinking, and oxidation induction period. It is widely used to characterize a wide variety of materials, including polymers, rubber, textiles, food, pharmaceuticals, and cosmetics.
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Equipment Description:

Differential Scanning Calorimetry (DSC), a classic thermal analysis method that studies thermal effects at programmable temperatures, has long been widely used in various fields of materials and chemistry, including research and development, process optimization, quality control, and failure analysis. Using DSC, we can study phase transitions in inorganic materials, the melting and crystallization processes of polymers, the polymorphism of pharmaceuticals, and the solid/liquid ratio of foods such as oils and fats.

Equipment Features:

1. The integrated design reduces signal loss and interference, significantly improving signal sensitivity and resolution, and achieving a more stable baseline.

2. Equipped with an imported high-frequency core control processor, it boasts faster processing speeds and more efficient control.

3. Utilizes imported high-sensitivity sensors, effectively improving DSC signal sensitivity and accuracy.

4. Independent atmosphere control, intelligently configured through software, allows the instrument to automatically switch gas flow systems, resulting in higher experimental efficiency.

5. Both the lower and upper controllers of the system feature multi-point temperature calibration, meeting the needs of various experimental scenarios and improving temperature measurement accuracy.

6. With two optional experimental modes, FTC and STC, temperature control is more user-friendly and flexible, meeting the needs of diverse experimental scenarios. This provides more precise temperature control during the experiment and more efficient analysis of sensor signals.

7. The fully controlled temperature system utilizes an optimized adaptive dynamic PID algorithm, significantly eliminating the manual adjustment requirements of traditional PID algorithms and enhancing the robustness of dual-mode temperature control. 8. 12-step programmable temperature control allows for more diverse experimental methods.

9. The sensor signal sampling frequency can be set from 1 to 10 Hz, providing greater flexibility in experimental methods and greater control over data.

10. Dual independent temperature sensors allow for simultaneous measurement of furnace and sample temperatures.

11. The system can perform heating, cooling, and isothermal material experiments.

12. The instrument utilizes bidirectional USB communication with self-healing connections. Its intelligent software features baseline subtraction, automatic plotting during the experiment, and intelligent data processing, including calculations of enthalpy, glass transition temperature, oxidation induction period, melting point, and crystallization.

Reference Standards:

1. GB/T 19466.2 – 2004 / ISO 11357-2: 1999 Part 2: Determination of glass transition temperature;

2. GB/T 19466.3 – 2004 / ISO 11357-3: 1999 Part 3: Determination of melting and crystallization temperatures and enthalpies;

3. GB/T 19466.6- 2009 / ISO 11357-3: 1999 Part 6: Oxidation induction period - Determination of oxidation induction time (isothermal OIT) and oxidation induction temperature (kinetic OIT).

DSC range 0-±2000mW
Timer frequency 16.6Hz
Temperature accuracy 0.001°C
Temperature fluctuation ±0.01°C
DSC noise 0.001mW
DSC accuracy 0.001mW
Experimental mode Optional FTC and STC settings
Programmed temperature control Flexible 12-step temperature control
Temperature control method Heating, constant temperature, cooling
Scan type Heating, cooling, isothermal scanning
Atmosphere control Two atmosphere settings, automatic switching
Display mode 24-bit color 7-inch LCD touchscreen display
Data interface Standard USB port
Sampling rate 1-10Hz programmable
Instrument calibration Multi-point temperature calibration function for both the lower and upper units
Parameter standards Supplied with standard materials for user-defined temperature and enthalpy correction
Instrument dimensions Dimensions: 490*390*215mm
Temperature range Room temperature to 600°C
Heating rate 0.1-100°C/min
Temperature resolution 0.01°C
Temperature repeatability ±0.01°C
DSC resolution 0.01μW
DSC sensitivity 0.001mW

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